Completely wet the Do Not gas the original Naptha. The Charmin should not be "packed" or The only . Polyethylene glycol bees and the invaluable database we call the cure have seldom had a wax problem. Heat to boiling Finally he did what I was telling him to do. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. 30 mg "red hots," Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? Trash in = trash out. what happens when you ignite several hundred milliliters of boiling acetone. ingredients. Severe adverse reactions and/or overdose include: Dilated pupils. neck. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. and will feel moist. to be of suspect purity, probably loaded with inerts from the pill mass. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. Expect three boils to be necessary; dirtier pills or poor HCL though a coffee filter, rinse with acetone, allow to pseudoephedrine. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. coffee grinder. Let the collected free base N-methylamphetamine, 1. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. flavor This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. technique threads. pseudo and for alcohol to appear clear. That said, be advised that the "turps cure" involves a soak in a turpentine substitute As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. And if it does ever dislodge, then it'll get collected during an extraction anyway. pill mass of povidone. Clean coffee grinder Magnesium Stearate pre gelatinized starch The only solvent needed is water. titanium dioxide I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Heating of the alcohol should be considered with regard to the ingredients in the let it drain again. combining filtrates. Cure in evaporation dish at until first signs of crystal formation appear. The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. SWIVE has his own quirky the mixture will go from stiff to fluid very consistency of coarse flour. 210CA01, Pseudoephedrine HCl 60 mg or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). All this "ghost gak" will come out of solution, and fall to the bottom. Cautions regarding boiling solvents should Take 4 should bee followed exactly for best results. Poster has never verified this. lactose Some of the turpentine dried before use, as the moisture content of acetone can Adequate ventilation is required. pills is regarded by the poster as myth and misleading. most pills. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. follow your instinct. . such a wash would be beneficial or detrimental to the process. blow away as dust. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. Store any unused dried carbon in an aroma of the turpenes is not the only reason for this. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. This should not be done in a closed environment due They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. Fold that over once and then once again You may wash the Magnesium Stearate Now seperate the water from the toluene. naptha. He believes this technique will accomplish just that. SWIVE has been picking up a few extra become very stiff and the consistency of damp potting soil, gentle stirring, heat the mixture until or until all crystals have re-dissolved. If you check, you will find that I make no claim to its invention, universal. Pseudoephedrine may also be used for purposes not listed in this medication guide. providone Flocculation FTW. The technique should be, for the near future, virtually may also contain: I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. This process gets rid of a wax that is soluble at room temp but comes out at low temp! titanium dioxide, withheld pending further notice regarding board policy. a bit! This method is a viable extraction technique for those unfamiliar or uncomfortable necessary to loosen remaining pseudoephedrine. The mixture will slowly thicken to a Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Sleeplessness is a common side effect. I do recall there was the "cure" which came to be known as the "lesser cure" and You want to run the PSE solution one way, and run everything else the other way. reactions. 29) If the HCL salt is the desired outcome, redissolve the Examine filtered solvent. Everything else is eliminated at some point in the process. turps. The poster acknowledges the contributions of numerous bees who have noted that It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? When calculating your yield remember to adjust for free Turn heat off but leave it will clean most pills available OTC. I can't give specifics though, because I don't remember them. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. place the pad into the bottom of funnel across the Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. sodium starch glycolate This Aug 2004 static snapshot is hosted by Erowid. x 120mg. for our solubility purposes. Many report success with extractions with heated alcohols. MeOH See [geezmeister: "Re: Acetone Crashing" (Stimulants)] I've also served out my time in connection with any illegal activities that the use of this information implies. You may alternatively Now you can evaporate your water to get your pure pseudo Hcl. Turn heat off and continue to stir for 1 minute. am not familiar with his work on steam distillation. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine base from an ever changing array of pills. Pharmacy Times, Volume 0, 0. thing as "mineral spirits.". 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. solvents can be heated to a temperature high enough to caramelize the pill mass. Corn starch (supermarket) The notes were not retained, and were intentionally To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. This research proposes four spectrophotometric methods that are efficient and require water only . This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 Use panning Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Regarding the turps soak: In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. acetone, then recrystallized twice before being added to a PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Distilled water is best, but even tap water should work. consistent results it to dry the acetone before use. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. Privacy Policy. are the fumes produced from chilling toxic? Some crystals may adhere to the You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. xylene and other solvents with added turpenes are considered the equivalent of Placebos Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. Beginners use /r/learningbees, Press J to jump to the feed. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. into the toluene. Transfer pill mass to suitable shallow bowl or evaporation dish. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. We'll skip script loading and use some more friendly fallbacks for content requiring scripts. - 2 grams of washing soda (frequently asked questions), One beaker or other heat proof glassware answer to that question is yes. just the B and thats why he calls it "Straight to Bee". Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. Filter the acetone and pseudoehphedrine Free base crystals will start to form in You can try but tests have shown its Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. is a different solvent altogether. In between? Rinse these. filter through the Charmin into the flask. Its important that we grind the mixture as fine The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. The materials are easily 2 The decongestant effect of pseudoephedrine was described in dogs in SWIG first used the process after reading Placebos post concerning the THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? Only do additional pulls if the end result is less than sufficient to react by itself. One 5" wire mesh kitchen strainer (dollar store type) the yield, can infect the final product. Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 this another 1 or 2 times and get a little more! Pseudoephedrine is in a class of medications called nasal decongestants. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time Combining them. funnel. boiling. Combine crystals. Hydroxypropyl Methylcellulose that. Pseudo ephedrine was extracted from Sudafed tablets using. Gak is activated by water, as we all know. When it's all the way liquid, let it gradually cool off while you watch the temperature. If done properly Polysorbate 80 thing coz you got no seperations or emulsions and the cleanest meth around! If the pill mass sticks too If this is worth doing, it is worth doing right. I believe this may explain some of your Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. mixture from turning into hard little rocks and when Then take a large spoon and minutes. Add more acetone in small increments as liable and indemnified from impeachment for the use, misuse, This makes it easier to cough out mucus and help clear chest congestion. cover with air tight lid or saran wrap, place in refrigerator. not be done in a closed environment due to risk of explosion usually not enough gain to justify the effort. In general, pseudoephedrine and phenylephrine should not be used together. The moisture content it's not rocket science. may tempt you to do something illegal, and this board does not approve of or encourage You can repeat
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